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A Comprehensive Textbook of Modern Pharmaceutical Analytical Techniques is a meticulously crafted academic resource designed to meet the growing demands of postgraduate students, researchers, and professionals in the field of pharmaceutical sciences. Aligned with the latest Pharmacy Council of India (PCI) curriculum for M. Pharm programs, this textbook presents a unified and in-depth understanding of modern instrumental and analytical methodologies used in drug discovery, quality control, formulation analysis, and regulatory compliance. What sets this textbook apart is its clarity, scientific depth, and pedagogical approach. It integrates insights from leading scientific literature, pharmacopeias (IP, BP, USP, EP), international guidelines, and recent trends in analytical instrumentation. Furthermore, the book includes over 100 cited references from authoritative sources such as B.K. Sharma, Skoog & Holler, P.D. Sethi, Willard, and others, providing a rich academic foundation for further exploration.