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As per new PCI Syllabus. This book provides guidelines to the students about Principle, Instrumentation and Applications of Nuclear Magnetic Resonance Spectroscopy, Mass Spectrometry, X-Ray Diffraction Methods, Thermal methods of analysis etc. Different advancements in the field of Spectroscopy and Chromatography have impacted the field of Pharmaceutical Analysis. Hypenetated techniques like GC-MS, LC-MS and HPTLC-MS are used for separation and analysis of different drugs. This book also imparts advanced knowledge to the students on the principle and instrumentation of these hyphenated techniques. The book Contains questions for evaluation And MCQs