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This textbook has been specifically developed on the directives of National Education Policy (NEP 2020) and is as per latest curriculum of B. Sc. Chemistry (Fifth Semester) for the Universities of Uttar Pradesh. Maintaining the traditional approach to the subject, Theory part comprehensively covers important topics such as Rearrangements, Catalysis, Main Group Elements, Transition Elements, Lanthanides, Actinides, Metal Carbonyls and Bioinorganic Chemistry. Practical Part covers Inorganic Qualitative Analysis, Analysis of Acid Radicals, Interference Among Acid Radicals, Analysis of Basic Radicals, Semi-Micro Analysis presented systematically to help students in achieving solid conceptional understanding and learn experimental procedures.