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This book, Instrumental Methods of Analysis, is designed to meet the growing demand for comprehensive knowledge of modern analytical instruments and their applications. It aims to provide students, researchers, and professionals with a clear understanding of the fundamental principles, instrumentation, and applications of various analytical techniques. The text begins by introducing basic concepts related to measurement and analysis, followed by detailed discussions of classical and modern techniques such as spectroscopy, chromatography, mass spectrometry, electroanalytical methods, and thermal analysis. Each chapter is supplemented with examples, illustrations, and real-world applications to provide practical insights into the functioning and utility of these instruments.