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This book is a guide for undergraduate and post graduate students. Many students do not have a good background of organic chemistry aswell as basics of spectroscopy. This examination oriented study guide book is written with these students in mind. this book will help studentsto overcome the fear of spectroscopy problemsthis guide book wwill help students to cover important concept, short answer questions, problems related to ultra violet, infrared, nuclear magnectic resonance as well as mass spectroscopy.